Senior Researcher
Research Center for Rheology and Non-Newtonian Fluids – CERNN
Federal University of Technology Parana – UTFPR
B.Sc. in Mechanical Engineering (UNOESC), M.Sc., Ph.D. in Mechanical and Materials Engineering (UTFPR)
nezia@funtefpr.org.br | +55 41 98748-2188
ORCID: 0000-0001-7210-9783
Research interests are in the general area of complex fluids, with a focus on rheology and petroleum engineering applications. In recent work, I have expanded into interfacial phenomena, especially how interfacial tension and wettability control emulsion stability and influence enhanced oil recovery (EOR). My work integrates numerical and experimental approaches, including Euler–Euler CFD and field-representative test rigs, to address challenges in drilling hydraulics, fluid displacement (cementing hydraulics), and flow assurance, with emphasis on transient pressure transmission and restart of gelled/paraffinic systems.
Methods/Tools: Rheology (non-Newtonian fluids and suspensions); field-representative flowloop/annular rigs; transient Euler–Euler CFD; LabVIEW for instrumentation/DAQ.
Highlighted achievements:
• Reduced drilling days from 96 to 44 (-52 days, ∼54%) by developing a model that predicts drillstring movement forces in the presence of cuttings, enabling faster well-hydraulics planning and mitigation of drag/stuck-pipe risks.
• Quantified the impact of temperature, cooling rate, and flow rate on the restartpressure peak in waxy-crude oil flow by designing and constructing a 50-m flow-loop experiment under field-representative operating conditions, showing up to 11.5× variation in restart pressure (+1050%) depending on operating conditions.
• Increased primary cementing displacement efficiency, showing turbulent flow tends to deliver 𝛼₂ ∼ 1 across 𝑅𝑒 ≈ 3.1 × 102
to 1.5 × 104, by leading largescale annular fluid-displacement experiments and mapping performance versus density ratio, viscosity ratio, and eccentricity (17% vs 60%), identifying density ratio as the dominant control parameter.
• Quantified apparent/relative viscosity evolution in Herschel–Bulkley non-colloidal suspensions as a function of Plastic number and Reynolds number, showing an exponential viscosity increase with Plastic number and a faster time-dependent viscosity decay at higher Reynolds numbers due to accelerated sedimentation, using a validated Euler–Euler CFD model for parallel-plate rheometry.
• Established safe viscosity-measurement limitsfor non-colloidal suspensions by identifying a critical modified Reynolds number (𝑅𝑒mod ∼ 10−³ ) where apparent viscosity approaches the homogeneous value, using transient Euler–Euler CFD across different geometries (cone-and-plate, parallel-plate, concentric cylinder; CP/PP/CC) (showing ≤5% 1-h deviation in CC vs. up to 60% in CP).
• Quantified the impact of NaCl and CaCl₂ brines on pressure transmission and restart pressures of paraffin- and olefin-based drilling fluids, showing that CaCl₂-based systems exhibit higher restart pressures and stronger time dependence.
Ongoing projects:
• Formulating a lightweight synthetic oil-based drilling fluid, reducing density from 8.8 to ∼6.0 ppg (−2.8 ppg, ∼32%) by incorporating low-density particles (e.g., hollow microspheres) and novel thickening agents to optimize stabilization, while maintaining rheological performance.
• Formulating a lightweight water-based drilling fluid, reducing density from 9.5 to ∼7.3 ppg (−2.2 ppg, ∼23%) by incorporating low-density particles (e.g., hollow microspheres) and sustainable plant-based fibers, and optimizing dispersion/stabilization, while maintaining rheological performance.
• Investigating the effect of crude-oil shrinkage on restart pressures, benchmarking flow-loop observations against laboratory rheology to improve field-to-lab scaling and prediction of restart behavior.
• Studying paraffin-in-oil emulsion stability as a function of interfacial tension, by varying surfactants and relating interfacial-tension measurements to separation kinetics and droplet coalescence in waxy systems.
• Investigating how oil phase composition and emulsifier (surfactant) chemistry govern the stability of essential-oil emulsions, quantifying changes in rheology and linking them to droplet-size distribution and destabilization mechanisms (e.g., coalescence/creaming).
• Increased refined soybean oil throughput from 282 to 313 t/day (+31 t/day, ∼11%) by optimizing operating conditions and coordinating shift execution.
• Achieved zero accidents by leading HSE execution across shifts, ensuring safe work planning and conducting incident/near-miss investigations with corrective actions.
• Ensured continuous monitoring and ocumentation of soybean oil extraction and soybean meal, refined soybean oil, and utilities throughout the full production cycle by serving as Quality & Environment Production Supervisor.
• Planned and executed scheduled shutdowns and maintenance, managing contractor interfaces, start-up preparation, and safe commissioning activities, ensuring all shutdowns were completed as planned, and the units were ready to return to production on schedule.
• Led Management of Change updating Standard Operating Procedures, training teams on changes, and maintaining documentation for compliance and audits. Achieved strong audit results, meeting or exceeding required standards.
The accretion of ice on aircraft wings, sensors, and engines presents a serious hazard to flight safety, underscoring the need for durable and energy-efficient ice protection strategies. Among emerging strategies, porous icephobic surfaces (PISs) have attracted considerable research interest due to the favorable durability, excellent icephobic performance, and low energy requirements. Nevertheless, critical aspects such as design objectives, theoretical foundations, fabrication techniques, and durability test standards for PISs have not yet been systematically examined, resulting in unclear research directions and motivating this review. This article first provides a comprehensive overview of existing aircraft ice protection strategies, establishing a broader context for the development of PIS. Through extensive literature analysis, the review then identifies contact angle hysteresis and icephobic durability as two key design parameters for PISs. Foundational principles related to lubricant transport, heat transfer, and wetting behavior in porous media are also introduced to furnish a solid theoretical basis for PIS design. Subsequently, slippery liquid-infused porous surfaces (SLIPS) are discussed as a prominent and successful example of PIS in ice protection applications, covering their fabrication methods, failure modes, and icing characteristics. However, SLIPS are prone to lubricant depletion under shear flow and rain erosion, which can substantially compromise their icephobic performance. Recent advances in PIS design have therefore incorporated strategies such as antifreeze agent release, lubricant replenishment, and covalent anchoring to reduce lubricant loss and enhance durability. To bridge the gap between simplified laboratory durability tests and the multifaceted testing required for aeronautical applications, this review outlines essential durability evaluation protocols for aeronautical implementation. Furthermore, the potential of artificial intelligence (AI) in accelerating the development and optimization of PIS is explored. Beyond offering a thorough synthesis of recent progress in PIS technology for anti-icing, this work also highlights PIS as a promising next-generation, durable, and energy-efficient candidate for aircraft ice protection.
Xanthan gum (XG) is a biopolymer used in various industries as a thickener and stabilizer. However, its tendency to agglomerate and form lumps during dispersion in water is an industry issue. The present work investigates the effect of ethanol acting as an XG dispersant in an aqueous solution and whether the dispersant affects the solution´s stability and rheological properties. The study proposes different concentrations of XG (0.1 %, 0.5 %, and 1 % wt) dissolved in water and an ethanol-water mixture. The results show that ethanol promotes faster and more effective hydration and dispersion of xanthan gum. This effect is particularly evident at intermediate (0.5 wt%) and high (1.0 wt%) concentrations, where the observed increase in viscosity suggests improved initial dispersion and enhanced rheological stability over time. The FTIR analysis indicates that ethanol disrupts hydrogen bonds, promotes polymer-polymer interactions, and increases dispersion homogeneity. Additionally, the zeta potential shows that ethanol increased the electrostatic stability of XG dispersions by augmenting the particles´ repulsion and thus preventing clustering, which results in more stable systems than water-alone solutions. The TGA analysis revealed that ethanol slightly enlarged the thermal stability of XG solutions due to stronger polymer-polymer interactions. Therefore, ethanol is an efficient, accessible, and environmentally friendly dispersant for improving XG dissolution, reducing processing time, and showing promising potential for industrial applications.
This study presents an experimental investigation into the startup flow of waxy crude oils in pipelines. An experimental rig was assembled with two syringe pumps connected to a 56.6-meter-long pipeline with an internal diameter of 10.3 mm. The experimental setup was placed within a thermal chamber to control the system temperature. The system was able to control thermal and shear history. The primary objective was to evaluate the start-up pressure required when initiating flow at a constant inlet flow rate. Unlike most prior works in the open literature, which discuss the rheological properties of crude oils at low temperatures, the current work explores the effect of the shear history, initial cooling temperature, aging time, and final cooling temperature in a startup flow loop. We also show in a pioneering experimental analysis that pressurizing the pipeline during the cooling evinces the effect of compressibility due to shrinkage on the startup of waxy crude oil.
This work investigates transient non-colloidal suspension flows in cone-and-plate, plate-plate, and cylindrical geometries to assess particle motion’s impact on viscosity measurement. Mass and momentum conservation equations model the two-phase liquid–solid flow, with both phases treated as continuous in an Euler-Euler approach. Findings demonstrate rheometric flow induces particle motion, affecting suspension homogeneity and viscosity measurement over time. Both buoyancy and inertia effects drive particle motion, with buoyancy dominating at low shear rates and inertia at high shear rates. Particle volume fractions, shear rates, and liquid viscosity notably influence viscosity measurements. Measurements with concentric cylinders are the least affected by particle motion. Additionally, we propose a time limit and a critical Reynolds number in which particle motion does not affect the measurement of the suspension viscosity.
This work aims at modeling the forces acting on the drill string assembly during its pull-out from the hole. Such forces arise from the interaction between equipment and both the cuttings bed and the well walls. The model is based on the continuity and momentum equations and the interactions with the cuttings bed are determined using concepts of granular materials. Comparisons with laboratory experimental data show the forces computed by the model are similar to that observed experimentally for different cuttings bed heights and drill bit areas. In addition, the model is able to predict whether a plug is formed or not. Finally, a case study was carried out by coupling the proposed model to an existing drag model to show the model’s potential for the detection of field problems.
The current work puts forward a numerical study of non-colloidal suspension flows in a parallel-plate geometry. The inhomogeneous Euler-Euler model applied to the continuity and momentum equations is used to solve the two-phase flow problem. The aim is at the investigation of particle motion in the suspensions flow and its consequence on the measured apparent viscosity. In contrast with prior works that dealt with neutrally buoyant flows, buoyancy is now taken into account. Good agreement was obtained between measured and computed particle distributions. Analysis of this distribution reveals that not only the particle motion but also the apparent viscosity depends on whether the lower or the upper plate is rotating. Comparisons between buoyant and non-buoyant flows were performed to understand the reasons behind the particle motion. Numerical experiments were conducted by rotating the upper or lower parallel plates and varying Reynolds number, particle volume fraction, density ratio and particle size. It can be anticipated that the particle motion in buoyant flows is mainly driven by a combination of gravity and a secondary flow perpendicular to the main circumferential flow.
I study the linear and nonlinear rheology of non-Newtonian and time-dependent fluids, including hydrogels, suspensions, emulsions, and de-icing formulations. My research focuses on how viscoelasticity, yield stress, and shear-dependent viscosity govern material response during flow, transport, and structural evolution under realistic operating conditions. Across these systems, I link microstructural dynamics to macroscopic flow behavior, establishing a mechanics-based framework for materials subjected to transient forcing, multiphase interactions, and application-relevant environments.
I investigate multiphase flows where interfacial phenomena and non-Newtonian rheology jointly determine performance, with emphasis on emulsions and suspensions relevant to petroleum engineering. I focus on the competition between interfacial tension/wettability and bulk effects—especially viscoplastic yield stress, viscoelasticity, and thixotropy—and how it governs breakup/coalescence, phase inversion, migration and segregation (creaming/sedimentation), and shear-induced structuring. My aim is to connect microstructure to flow metrics such as pressure losses, transport capacity, and separation times under transient and field-relevant conditions, spanning drilling/completion, flow assurance, and related industrial systems.
I investigate interfacial phenomena—especially how interfacial tension and wettability control emulsion stability and influence enhanced oil recovery (EOR). My focus is on the interplay between surface/interfacial forces and non-Newtonian rheology, connecting interfacial properties to macroscopic outcomes such as stability, separation kinetics, and flow performance in petroleum-relevant multiphase systems. A central thread of my current work is understanding waxy (paraffin-in-oil) emulsions, where I vary surfactant chemistry and directly relate interfacial-tension measurements to droplet coalescence and phase separation kinetics. In parallel, I study how oil-phase composition and emulsifier selection govern emulsion stability, linking droplet-size distributions and destabilization routes (e.g., coalescence/creaming) to measurable rheological changes.
I employ transient CFD to analyze and predict the behavior of complex, non-Newtonian multiphase flows, with particular emphasis on systems in which rheology, phase distribution, and loading history jointly govern performance. My work integrates viscoplastic (yield-stress) and time-dependent constitutive models within Euler–Euler multiphase frameworks and is tightly coupled with experimental observations to ensure physical fidelity and field relevance. I develop and validate CFD models of rotational rheometric geometries (e.g., parallel-plate, cone-and-plate, and concentric cylinder) to quantify how spatial heterogeneity, sedimentation, and shear history bias apparent viscosity measurements in non-colloidal suspensions. These insights are then translated to engineering-scale predictions, enabling more reliable estimates of pressure losses, restart and pressure transmission behavior, suspension stability and segregation, and displacement and transport efficiency in applications such as drilling and completion fluids, waxy/crude oil restart flows, and annular cementing hydraulics.
– Akanksha Gavendra (Ph.D. student, 2025–)Influence of Surfactants on Waxy Paraffinin-Oil Emulsion Rheology.
– Nahyan Tiego Pagliatto de Liz (Ph.D. student, 2025–) Droplet-Size–Rheology Links in Essential-Oil Emulsion Destabilization.
– Fabian Leonardo Ramos Maldonado (M.Sc. student, 2024–) Formulation and Characterization of Lightweight Water-Based Drilling Fluids Using Alternative Microparticles.
– Maria Isabel Hernández Montoya (B.Sc. student, 2024–) Formulation and Rheological Characterization of a Low-Density Water-Based Drilling Fluid.
– Andrew O. Ogundele (B.Sc. student, 2025–) Mathematical and Numerical Modelling of the Influence of Hydrogel Rheology on Filament Formation and Printability in Extrusion-Based 3D Printing.
– Ana Murta (B.Sc. student, 2025–) Rheological Characterization of Petroleum TankBottom Sludge.
– Abraão Braga da Silva (B.Sc. student, 2025–) Instrumented Rheometry for Drilling Fluids: Real-Time Local Normal/Shear Stress Mapping.
– Maicon José (B.Sc. student, 2025–) Experimental Evaluation of the Effect of Paraffinic Oil Shrinkage on Flow-Restart Pressure.
– Kaio Matheus Barros de Oliveira (B.Sc. student, 2025–) Influence of Surfactants on the Stability of Paraffinic Emulsions.
– Felipe Miranda (B.Sc. student, 2025–) Design of an Experimental Rig to Evaluate the Effect of Pipe Roughness on the Flow-Restart Pressure of Crude Oil.
– Patricia Vieira de Oliveira (Postdoctoral Fellow, 2024–2025) Lightweight Synthetic Oil-Based Drilling Fluid Formulation (8.8 to ∼6.0 ppg) Using Low-Density Particles.
– Giovanni Paolo Montagnoli (M.Sc. student, 2022–2025) Modeling of Two-Phase Liquid–Gas Flow in a Hydrogen Production Cell. Currently at Rheology Group (GREO), Brazil.
– Mateus Debiase (M.Sc. student, 2018–2021) Experimental Evaluation of Cuttings Displacement by the Drill Bit–Drill String Assembly in a Horizontal Well. Currently at Irani Celulose, Brazil.
– Maryelen Hissae Miyoshi (M.Sc. student, 2017–2020) Modeling the Displacement of the Drill String Immersed in a Cuttings Bed. Currently at Prysmian, Italy.
– Denis Barbara Barbosa (B.Sc. student, 2023–2025) Numerical Investigation of Shrinkage Dynamics During Paraffin-Wax Phase Transition.
– Renan Seidel (B.Sc. student, 2021–2023) Development of a Device to Evaluate Drilling-Fluid Compressibility. Currently at Volvo, Sweden.
– Gabriel Gianesini (B.Sc. student, 2021–2022) Experimental Evaluation of Pressure Variations During Drill-String Movement. Currently at Volvo, Brazil.
– Fernando Gbur Mazzuchetti (B.Sc. student, 2020–2022) Experimental Evaluation of the Effect of Drill-String Rotation on Pressure Transmission. Currently at Volvo, Brazil.
– Marcio Giacomello (B.Sc. student, 2019–2021) Experimental Evaluation of Fluid Displacement in Primary Cementing. Currently at Volvo, Brazil.
– Sophia Roennfeldt (B.Sc. student, 2019–2021) Experimental Evaluation of DrillString Displacement in the Presence of Cuttings. Currently at Volvo, Brazil.
– Otávio Augusto Verhagem (B.Sc. student, 2018–2021) Numerical Evaluation of Fluid Displacement in Primary Cementing. Currently at TotalEnergies, France.
– Gabriela Tuca Palma (B.Sc. student, 2021) Experimental Evaluation of Drill-String Displacement in the Presence of Cuttings. Currently at Volvo, Brazil.
– Julio Jorge de Almeida Abdala (B.Sc. student, 2017–2022) Experimental Evaluation of Drilling-Fluid Compressibility. Currently at FUNTEF/UTFPR, Brazil.
– Isabela Rocha (B.Sc. student, 2018) Rheological Characterization of Non-Colloidal Suspensions. Currently at Renault, Brazil.
– Maryelen Hissae Miyoshi (B.Sc. student, 2016–2017) Modeling the Displacement of a Solid Boundary in a Solid–Liquid Medium. Currently at Prysmian, Italy.
– Gabriel Tanaka Nunes (B.Sc. student, 2017–2018) Experimental Study of Flow Restart in Thixotropic Fluids. Currently at Hexagon Manufacturing Intelligence, Belgium.
– Rodrigo Mitishita (B.Sc. student, 2015–2017) Experimental Study of Pressure Transmission in Drilling Fluids. Currently at Coanda Research & Development, Canada.
– Fernando Kroetz (B.Sc. student, 2015–2017) Experimental Study of Crude-Oil Flow Restart. Currently at Synospe, Brazil.
• ME76G – Heat Transfer I (2020), 18 students.
• PDC99 – Rheology and Rheometry (2024–2025), 23 and 21 students.
• Invited lecture at UTFPR Curitiba (Industrial Processes 2, B.Sc. Chemistry), “Industrial Soybean Oil Extraction Process”, Academic Department of Chemistry and Biology, Federal University of Technology of Paraná, Curitiba, Brazil, Feb. 4, 2025 (3 h).
• Invited Speaker at SPE Brazil Tech Tuesday, “Estimating Fluid Contamination during Well Cementing” (talk delivered in Portuguese: “Estimativa da Contaminação de Fluidos durante a Cimentação de Poços”), May 24, 2022.
A R2 contrata um projeto de PD&I com o grupo de pesquisa da ICT’s, se for necessário através das fundações de apoio, para pagamentos da equipe.
Reviewer for peer-reviewed journals, including:
• Geoenergy Science and Engineering
• Journal of the Brazilian Society of Mechanical Sciences and Engineering
• Organizer committee the 20th Brazilian Congress of Thermal Sciences and Engineering (ENCIT), Iguazu Falls, Brazil, 2024.
• Organizer committee the IX National Meeting on Oil & GasWell Construction (ENAHPE), Matinhos, Brazil, 2023.
• Organizer committee the VII Brazilian Conference on Rheology (BCR), Curitiba, Brazil, 2015.
I have also served as Session Chair for various conferences in recent years, including OTC Brasil, the Brazilian Congress of Thermal Sciences and Engineering (ENCIT), the International Congress of Mechanical Engineering (COBEM), the Brazilian Conference on Rheology (BCR), and Colloids 2025.
Reviewer for entrepreneurship and innovation incubation applications, including SprinT (UTFPR’s incubator), supporting the evaluation of technology-based ventures throughout the incubation
process (e.g., management, technology, market, capital, and entrepreneurship criteria).
Petrobras: consulting on problems associated with restarting the flow of gelled/paraffinic crude
oils, 2022.
• Lima, G. D. S. V.; Negrão, C. O. R.; de Rosso, N.; Barreira, E. M.; Kroetz, F. M.; Carvalho, P. H. Auxiliary System and Method for Starting or Restarting the Flow of Gelled Fluid. United States. USPTO (Privilégio de Inovação), US2021/0356080, granted Nov. 10, 2021.
• Kroetz, F. M.; Negrão, C. O. R.; de Rosso, N.; Carvalho, P. H.; Barreira, E. M.
Method for Restarting the Flow of Gelled Fluids. Brazil. INPI (Privilégio de Inovação), BR1020160190290, filed Aug. 17, 2016.
• Martins, A. L.; Waldmann, A. T. A.; Sansoni Junior, U.; Filipak, D. J.; Miyoshi, M. H.; de Rosso, N.; Negrão, C. O. R. SAPP – Drag Simulator for Well Drilling (SAPP
• Simulador de Arraste na Perfuração de Poços). Brazil. INPI (Software/Computer Program), BR512022001876-4, registered Sep. 21, 2021.
Co-founded R2 Simulation, specializing in computational fluid dynamics (CFD) and advanced numerical simulation.
My research involves collaborations with UTFPR faculty and external academic and industry partners, including Prof. D. E. V. Andrade (UFRGS), Prof. M. Nele (UFRJ), Dr. A. Leihbson; Eng. A. T. A. Waldmann (Petrobras), and Prof. Z. Zhang (Beihang University).
• The Society of Rheology (SoR)
• Brazilian Society of Rheology (SBR)
• Brazilian Association of Engineering and Mechanical Sciences – ABCM
I have been an instructor for the Introduction to Rheology for Industrial Applications course.
This is a 3- to 4-day intensive course/workshop for industry participants. This year (2025), the course was offered at Iconic Lubricants in Duque de Caxias, Rio de Janeiro, Brazil.
• Member of the Multi-User Management Committee (LabREO), UTFPR, Brazil, 2016 – 2023.
• Member of the Communication Committee of the Brazilian Society of Rheology (SBR), since 2023.
UTFem Extension Program (UTFPR, Curitiba, Brazil) – Member, 2023–Present.
• I participate in a university extension initiative that strengthens a technology and knowledgedriven ecosystem for women’s entrepreneurship in STEAM, promoting innovation, knowledge transfer, and increased visibility of women-led research aligned with SDG 5 (Gender
Equality).